[en] Nowadays, due to their natural availability, renewability, biodegradability, nontoxicity, light weight and relatively low cost, natural fibers, especially lignocellulosic fibers, present attractive potential to substitute non-eco-friendly synthetic fibers. In this study, Ziziphus jujuba fibers were used, thanks to their low lignin content, as an alternative of renewable resource for the production of cellulosic fibers with suitable characteristics and minimal time and energy consumption. In fact, due to their valuable chemical composition, it was possible to remove the amorphous fractions and impurities from the fiber surface by applying ultrasounds coupled with alkaline treatment (80 °C, 5 wt.% NaOH), followed by a bleaching step. The efficient dissolution of the noncellulosic compounds was confirmed by Fourier Transform Infrared Spectroscopy (FTIR). The resulted increase in the crystallinity index (from 35.7% to 57.5%), occurred without impacting the crystalline structure of the fibers. The morphological analysis of the fibers evidences the higher surface area of the obtained fibers. Based on the obtained results, Ziziphus jujuba fibers were found to present a suitable sustainable source for the production of cellulosic fibers.
Disciplines :
Materials science & engineering
Author, co-author :
Amior, Aicha; Laboratoire LSPN, Université 8 Mai 1945 Guelma, BP 401, Guelma 24000, Algeria
Satha, Hamid; Laboratoire LSPN, Université 8 Mai 1945 Guelma, BP 401, Guelma 24000, Algeria
Laoutid, Fouad ; Université de Mons - UMONS > Unités externe > Materia Nova ASBL
Toncheva, Antoniya ; Université de Mons - UMONS > Unités externe > Materia Nova ASBL
DUBOIS, Philippe ; Université de Mons - UMONS > Faculté des Science > Service des Matériaux Polymères et Composites
Language :
English
Title :
Natural Cellulose from Ziziphus jujuba Fibers: Extraction and Characterization.
Siva R. Valarmathi T.N. Palanikumar K. Samrot A.V. Study on a novel natural cellulosic fiber from Kigelia africana fruit: Characterization and analysis Carbohydr. Polym. 2020 244 116494 10.1016/j.carbpol.2020.116494 32536404
Ramesh M. Palanikumar K. Reddy H.K. Plant fibre based bio-composites: Sustainable and renewable green materials Renew. Sustain. Energy Rev. 2017 79 558 584 10.1016/j.rser.2017.05.094
Ding L. Han X. Cao L. Chen Y. Ling Z. Han J. He S. Jiang S. Characterization of natural fiber from manau rattan (Calamus manan) as a potential reinforcement for polymer-based composites J. Bioresour. Bioprod. 2022 7 190 200 10.1016/j.jobab.2021.11.002
Satha H. Kouadri I. Benachour D. Thermal, Structural and Morphological Studies of Cellulose and Cellulose Nanofibers Extracted from Bitter Watermelon of the Cucurbitaceae Family J. Polym. Environ. 2020 28 1914 1920 10.1007/s10924-020-01735-6
Du H. Liu W. Zhang M. Si C. Zhang X. Li B. Cellulose nanocrystals and cellulose nanofibrils based hydrogels for biomedical applications Carbohydr. Polym. 2019 209 130 144 10.1016/j.carbpol.2019.01.020 30732792
Asif M. Ahmed D. Ahmad N. Qama M.T. Alruwaili N.K. Bukhari S.N.A. Extraction and characterization of microcrystalline cellulose from Lagenaria Siceraria fruit predicles Polymers 2022 14 1867 10.3390/polym14091867 35567035
Khandanlou R. Ngoh G.C. Chong W.T. Feasibility Study and Structural Analysis of Cellulose Isolated from Rice Husk: Microwave Irradiation, Optimization, and Treatment Process Scheme BioResources 2016 11 5751 5766 10.15376/biores.11.3.5751-5766
Melikoğlu A.Y. Bilek S.E. Cesur S. Optimum alkaline treatment parameters for the extraction of cellulose and production of cellulose nanocrystals from apple pomace Carbohydr. Polym. 2019 215 330 337 10.1016/j.carbpol.2019.03.103
Sai Prasanna N. Mitra J. Isolation and characterization of cellulose nanocrystals from Cucumis sativus peels Carbohydr. Polym. 2020 247 116706 10.1016/j.carbpol.2020.116706
Wang J. Han X. Zhang C. Liu K. Duan G. Source of Nanocellulose and Its Application in Nanocomposite Packaging Material: A Review Nanomaterials 2022 12 3158 10.3390/nano12183158
Han X. Ding L. Tian Z. Song Y. Xiong R. Zhang C. Han J. Jiang S. Potential new material for optical fiber: Preparation and characterization of transparent fiber based on natural cellulosic fiber and epoxy Int. J. Biol. Macromol. 2022 224 1236 1243 10.1016/j.ijbiomac.2022.10.209 36550788
Reshmy R. Philip E. Paul S.A. Madhavan A. Sindhu R. Binod P. Pandey A. Sirohi R. Nanocellulose-based products for sustainable applications–recent trends and possibilities Rev. Environ. Sci. Biotechnol. 2020 19 779 806 10.1007/s11157-020-09551-z
Adeli M. Samavati V. Studies on the steady shear flow behavior and chemical properties of water-soluble polysaccharide from Ziziphus lotus fruit Int. J. Biol. Macromol. 2015 72 580 587 10.1016/j.ijbiomac.2014.08.047 25195543
Basyony M.M. Elsheikh H.A. Abdel Salam H.S. Mohamed K.I. Zedan A.H. Utilization of ziziphus spina-christi leaves as a natural growth promoter in rabbit’s rations EJRS 2017 27 427 446 10.21608/ejrs.2017.46666
Hassainia A. Satha H. Boufi S. Chitin from Agaricus bisporus: Extraction and characterization Int. J. Biol. Macromol. 2018 117 1334 1342 10.1016/j.ijbiomac.2017.11.172
Hassainia A. Satha H. Boufi S. Two Routes to Produce Chitosan from Agaricus bisporus J. Renew. Mater. 2020 8 101 111 10.32604/jrm.2020.07725
Kouadri I. Satha H. Extraction and characterization of cellulose and cellulose nanofibers from Citrullus colocynthis seeds Ind Crops Prod. 2018 124 787 796 10.1016/j.indcrop.2018.08.051
Boureghda Y. Satha H. Bendebane F. Chitin–Glucan Complex from Pleurotus ostreatus Mushroom: Physicochemical Characterization and Comparison of Extraction Methods J. Waste Biomass Valorization 2021 12 6139 6153 10.1007/s12649-021-01449-3
Sluiter A. Determination of Structural Carbohydrates and Lignin in Biomass: Laboratory Analytical Procedure (LAP) National Renewable Energy Laboratory Golden, CO, USA 2011
Segal L. Creely L. Martin A.E. Conrad M. An empirical method for estimating the degree of crystallinity of native cellulose using the X-ray diffractometer Text. Res. J. 1958 29 786 794 10.1177/004051755902901003
Makhlouf A. Layachi A. Kouadri I. Belaadi A. Satha H. Structural study and thermal behavior of composites: Polyamide 66/glass fibers: The reinforcement ration effect on the kinetics of crystallization J. Compos. Mater. 2020 54 1467 1481 10.1177/0021998319883913
Maepa C.E. Jayaramudu J. Okonkwo J.O. Ray S.S. Sadiku E.R. Ramontja J. Extraction and characterization of natural cellulose fibers from maize tassel Int. J. Polym. Anal. Charact. 2015 20 99 109 10.1080/1023666X.2014.961118
Zhao G. Du J. Chen W. Pan M. Chen D. Preparation and thermostability of cellulose nanocrystals and nanofibrils from two sources of biomass: Rice straw and poplar wood Cellulose 2019 26 8625 8643 10.1007/s10570-019-02683-8
Fareez I.M. Ibrahim N.A. Yaacob W. Razali N.A.M. Jasni A.H. Aziz F.A. Characteristics of cellulose extracted from Josapine pineapple leaf fibre after alkali treatment followed by extensive bleaching Cellulose 2018 25 4407 4421 10.1007/s10570-018-1878-0
Yue Y. Han J. Han G. Aita G.M. Wu Q. Cellulose fibers isolated from energycane bagasse using alkaline and sodium chlorite treatments: Structural, chemical and thermal properties Ind. Crops Prod. 2015 76 355 363 10.1016/j.indcrop.2015.07.006
Sarikanat M. Seki Y. Sever K. Durmuskahya C. Determination of properties of Althaea officinalis L. (Marshmallow) fibers as a potential plant fiber in polymeric composite materials Compos. B. Eng. 2014 57 180 186 10.1016/j.compositesb.2013.09.041
Senthamaraikannan P. Saravanakumar S.S. Arthanarieswaran V.P. Sugumaran P. Physicochemical properties of new cellulosic fibers from bark of Acacia planifrons Int. J. Polym. Anal. Char. 2016 21 207 213 10.1080/1023666X.2016.1133138
Tanpichai S. Witayakran S. All-cellulose composite laminates prepared from pineapple leaf fibers treated with steam explosion and alkaline treatment J. Reinf. Plast. Compos. 2017 36 1146 1155 10.1177/0731684417704923
Vijay R. Manoharan S. Arjun S. Vinod A. Singaravelu D.L. Characterization of silane-treated and untreated natural fibers from stem of Leucasaspera J. Nat. Fibers 2020 18 1 17
Vinod A. Vijay R. Lenin Singaravelu D. Sanjay M.R. Siengchin S. Moure M.M. Characterization of untreated and alkali treated natural fibers extracted from the stem of Catharanthusroseus Mater. Res. Express. 2019 6 085406 10.1088/2053-1591/ab22d9
Khan A. Vijay R. Singaravelu D.L. Sanjay M.R. Siengchin S. Verpoort F. Alamry K.A. Asiri A.M. Extraction and characterization of natural fiber from eleusine indica grass as reinforcement of sustainable fiber-reinforced polymer composites J. Nat. Fibers 2019 18 1 9 10.1080/15440478.2019.1697993
Balaji A.N. Nagarajan K.J. Characterization of alkali treated and untreated new cellulosic fiber from Saharan Aloe vera cactus leaves Carbohydr. Polym. 2017 174 200 208
Reddy K.O. Ashok B. Reddy K.R.N. Feng Y.E. Zhang J. Rajulu A.V. Extraction and characterization of novel lignocellulosic fibers from Thespesia lampas plant Int. J. Polym. Anal. Char. 2014 19 48 61 10.1080/1023666X.2014.854520
Suryanto H. Marsyahyo E. Irawan Y.S. Soenoko R. Morphology, structure, and mechanical properties of natural cellulose fiber from mending grass (Fimbristylisglobulosa) J. Nat. Fibers 2014 11 333 351 10.1080/15440478.2013.879087
Fiore V. Scalici T. Valenza A. Characterization of a new natural fiber from Arundodonax L. as potential reinforcement of polymer composites Carbohydr. Polym. 2014 106 77 83 10.1016/j.carbpol.2014.02.016
Raja K. Prabu B. Ganeshan P. Chandra Sekar V.S. NagarajaGanesh B. Characterization studies of natural cellulosic fibers extracted from shwetark stem J. Nat. Fibers 2020 18 1 14 10.1080/15440478.2019.1710650
Ganapathy T. Sathiskumar R. Senthamaraikannan P. Saravanakumar S.S. Khan A. Characterization of raw and alkali treated new natural cellulosic fibres extracted from the aerial roots of banyan tree Int. J. Biol. Macromol. 2019 138 573 581 10.1016/j.ijbiomac.2019.07.136
Manimaran P. Saravanan S.P. Sanjay M.R. Siengchin S. Jawaid M. Khan A. Characterization of new cellulosic fiber: Dracaena reflexa as a reinforcement for polymer composite structures J. Mater. Res. Technol. 2019 8 1952 1963 10.1016/j.jmrt.2018.12.015
Moshi A.A.M. Ravindran D. Bharathi S.R.S. Indran S. Saravanakumar S.S. Liu Y. Characterization of a new cellulosic natural fiber extracted from the root of Ficus religiosa tree Int. J. Biol. Macromol. 2020 142 212 221 10.1016/j.ijbiomac.2019.09.094
Kommula V.P. Reddy K.O. Shukla M. Marwala T. Reddy E.V.S. Rajulu A.V. Extraction, modification, and characterization of natural ligno-cellulosic fiber strands from napier grass Int. J. Polym. Anal. Char. 2016 21 18 28 10.1080/1023666X.2015.1089650
Palacios Hinestroza H. Hernandez Diaz J.A. Esquivel Alfaro M. Toriz G. Rojas O.J. Sulbaran-Rangel B.C. Isolation and Characterization of Nanofibrillar Cellulose from Agave tequilana Weber Bagasse Adv. Mater. Sci. Eng. 2019 2019 1342547 10.1155/2019/1342547
Kozłowski R. Władyka-Przybylak M. Flammability and fire resistance of composites reinforced by natural fibers Polym. Adv. Technol. 2008 19 446 453 10.1002/pat.1135
Porras A. Maranon A. Ashcroft I.A. Characterization of a novel natural cellulose fabric from Manicariasaccifera palm as possible reinforcement of composite materials Compos. B. Eng. 2015 74 66 73 10.1016/j.compositesb.2014.12.033
Jothibasu S. Mohanamurugan S. Vinod A. Influence of chemical treatments on the mechanical characteristics of areca sheath flax fibres based epoxy composites J. Chem. 2018 11 1255 1262
Kouadri I. Layachi A. Makhlouf A. Satha H. Optimization of extraction process and characterization of water-soluble polysaccharide (Galactomannan) from Algerian biomass; Citrullus colocynthis seeds Int. J. Polym. Anal. Charact. 2018 23 362 375 10.1080/1023666X.2018.1455343
Khenblouche A. Bechki D. Gouamid M. Charradi K. Segni L. Hadjadj M. Boughali S. Extraction and characterization of cellulose microfibers from Retamaraetam stems Polímeros. 2019 29 1 8 10.1590/0104-1428.05218
Amior A. Kouadri I. Makhlouf A. Satha H. Extraction process of Galactomannan from Algerian biomass; optimization and physic-chemical analysis Proceedings of the Fifth International Conference on Biobased Materials and Composites: ICBMC Monastir, Tunisia 17–20 March 2019
Mohamed N.A.N. Jai J. Response surface methodology for optimization of cellulose extraction from banana stem using NaOH-EDTA for pulp and paper making Heliyon 2022 8 e09114 10.1016/j.heliyon.2022.e09114
Tanpichai S. Mekcham S. Kongwittaya C. Kiwijaroun W. Thongdonsun K. Thongdeelerd C. Boonmahitthisud A. Extraction of Nanofibrillated Cellulose from Water Hyacinth Using a High Speed Homogenizer J. Nat. Fibers 2021 19 5676 5696 10.1080/15440478.2021.1889432
Rohadi T.N.T. Ridzuan M.J.M. Majid M.S.A. Khasri A. Sulaiman M.H.J. Mater Res. Technol. 2020 9 15057 15071
Johar N. Ahmad I. Dufresne A. Extraction, preparation and characterization of cellulose fibres and nanocrystals from rice husk Ind. Crops Prod. 2012 37 93 99 10.1016/j.indcrop.2011.12.016
Saravanakumar S.S. Kumaravel A. Nagarajan T. Moorthy I.G. Investigation of physico-chemical properties of alkali-treated Prosopis juliflora fibers Int. J. Polym. Anal. Charact. 2014 19 309 317 10.1080/1023666X.2014.902527
Senthamaraikannan P. Kathiresan M. Characterization of raw and alkali treated new natural cellulosic fiber from Coccinia grandis L. Carbohydr. Polym. 2018 186 332 343 10.1016/j.carbpol.2018.01.072 29455994
Yue Y. Han J. Han G. Zhang Q. French A.D. Wu Q. Characterization of cellulose I/II hybrid fibers isolated from energycane bagasse during the delignification process: Morphology, crystallinity and percentage estimation Carbohydr. Polym. 2015 133 438 447 10.1016/j.carbpol.2015.07.058
Ciftci D. Flores R.A. Saldaña M.D.A. Cellulose fiber isolation and characterization from sweet blue lupin hull and canola straw J. Environ. Polym. Degrad. 2018 26 2773 2781 10.1007/s10924-017-1164-5
Bharathiraja B. Sudharsanaa T. Bharghavi A. Sowmeya G.S. Balaram G. Insights on lignocellulosic pretreatments for biofuel production-SEM and reduction of lignin analysis Int. J. ChemTech Res. 2014 6 4334 4444
Cullity B.D. Elements of X-ray Diffraction 2nd ed. Addison–Wesley New York, NY, USA 1978
NagarajaGanesh B. Ganeshan P. Ramshankar P. Raja K. Assessment of natural cellulose fibers derived from Sennaauriculata for making light weight industrial biocomposites Ind. Crops Prod. 2019 139 111546 10.1016/j.indcrop.2019.111546
Tanpichai S. Witayakran S. Srimarut Y. Woraprayote W. Malila Y. Porosity, density and mechanical properties of the paper of steam exploded bamboo microfibers controlled by nanofibrillated cellulose J. Mater. Res. Technol. 2019 8 3612 3622 10.1016/j.jmrt.2019.05.024
Khawas P. Deka S.C. Isolation and characterization of cellulose nanofibers from culinary banana peel using high-intensity ultrasonication combined with chemical treatment Carbohydr. Polym. 2016 137 608 616 10.1016/j.carbpol.2015.11.020
Brebu M. Vasile C. Thermal degradation of lignin—A review Cellul. Chem. Technol. 2010 44 353 363
Mouhoubi S. Bourahli M.E.H. Osmani H. Abdeslam S. Effect of alkali treatment on alfa fibers behavior J. Nat. Fibers 2017 14 239 249 10.1080/15440478.2016.1193088
Yan L. Chouw N. Yuan X.J. Experimental Investigation and Analysis of Mercerized and Citric Acid Surface Treated Bamboo Fiber Reinforced Composite Reinf. Plast. Compos. 2012 31 425 437 10.1177/0731684412439494
Kargarzadeh H. Ahmad I. Abdullah I. Dufresne A. Zainudin S.Y. Sheltami R.M. Effects of hydrolysis conditions on the morphology, crystallinity, and thermal stability of cellulose nanocrystals extracted from kenaf bast fibers Cellulose 2012 19 855 866 10.1007/s10570-012-9684-6
Ouarhim W. Essabir H. Bensalah M. Zari N. Bouhfid R. Structural laminated hybrid composites based on raffia and glass fibers: Effect of alkali treatment, mechanical and thermal properties Compos. B 2018 154 128 137 10.1016/j.compositesb.2018.08.004